中華民國內政部建築研究所中華民國內政部建築研究所

防火材料之品質攸關保障人民之安全，熱重分析法為可行有效的檢測方式之一，為進一步建置熱重分析設備，完善本所防火實驗中心熱分析檢測項目，以提供檢測服務及跨足材料研發的領域。
本案依據研究預期成果目標，各項研究成果結論如下：
（一）完成建立熱重分析相關設備與操作技術
本項設備已完成建置，設備性能經以標準件查驗符合要求，設備操作手冊（如附錄2），可供後續人員訓練及操作參考使用。
（二）收集與研析熱重分析試驗標準要求
我國CNS國家標準尚無相關熱重分析標準，而目前國內有TGA的TAF實驗室，主要試驗依據標準為ASTM E1131及ASTM D6370(橡膠類)，本研究主要參考ASTM E1131 、ISO 11358及GOST R 53293，供後續參考使用。
（三）初步建立防火材料熱分析基本數據
以本研究所取試樣試驗，其結果顯示較為均質的材料，其各次試驗結果再現性佳；但在組成為非均質且熱膨脹率高的試樣，其在加熱試驗過程試樣膨脹碰觸秤重裝置，無法反應其熱重性質，後續須針對此類試樣再加以探討。

The quality of fireproof materials is critical to the safety of the people. Thermogravimetric analysis is one of the feasible and effective detection methods. In order to further build thermogravimetric analysis equipment, improve the thermal analysis and testing projects of our fire experiment center to provide testing services and stepping into the field of material research and development.
The conclusions of the research results are as follows:
(1)Complete the establishment of thermogravimetric analysis related equipment and operating technology.
(2)There is no relevant thermogravimetric analysis standard for CNS standard. This research mainly refers to ASTM E1131, ISO 11358 and GOST R 53293 for subsequent reference.
(3)The test results of samples taken from this research show that for relatively homogeneous materials, the reproducibility of the results of each test is good; but for the samples with non-homogeneous composition and high thermal expansion rate, the samples expand and touch during the heating test. The weighing device cannot reflect its thermogravimetric properties, and it must be discussed later for this type of sample.